By Edited by Pietro VINCENZINI World Academy of Ceramics and National Research Council, Italy Co-edited by Michele DONDI CNR-ISTEC, Italy
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Additional info for 12th INTERNATIONAL CERAMICS CONGRESS PART G Proceedings of the 12 th International Ceramics Congress, part of CIMTEC 2010- 12 th International Ceramics Congress and 5th Forum on New Materials Montecatini Terme, Italy, June 6-11, 2010
A Vol. 465 (2009), p. 2407  S. Lee, Y. J. Kim and H. S. Moon: J. Amer. Ceram. Soc. Vol. 82 (1999), p. be, Keywords: Hybrid, lamellar, silica, templating, mesoporous, silane. Abstract. This paper is focused on the preparation and characterization of different lamellar silica prepared by liquid crystal templating and silanisation. The initial template can be removed and replaced in the interlamellar spaces by different types of silane, being covalently grafted to the solid by reaction with the surface silanols.
It must be emphasized that lattice parameters are always situated inside the orthorhombic mullite area presented by Okada for a large number of various mullite, (figure 3 in 12). 00 Fig. 4 : Lattice constants and cell volumes of mullite versus the thermal cycle, compared to the average data from 12. (a): a and b constants; (b) : c constant. ( ): 1100°C, 3°C/min; ( ): 1150°C, 3°C/min; ( ): 1100°C, 20°C/min; ( ): 1150°C, 20°C/min; ( ) :1100°C, 3°C/min, 12h; ( ) : 1100°C, 3°C/min, 12h. Table II shows a comparison made with samples, which were first sintered at both temperatures and temperature rates, but maintained at these temperatures for 12 hours.
They evidence a residual structural order of high temperature phases which is favorable to the topotactic recrystallization of mullite; (ii) from the high temperature form of phyllosilicates, an organized network of mullite can be obtained; (iii) the composition of a local and transient liquid and the presence of minor elements as Fe has a significant influence on the mullite morphology; (iv) mechanical properties are closely related to size and organization degree of the mullite network; (v) the process itself influence the kinetic of structural transformation and particularly the powder compact density and the thermal cycle.
12th INTERNATIONAL CERAMICS CONGRESS PART G Proceedings of the 12 th International Ceramics Congress, part of CIMTEC 2010- 12 th International Ceramics Congress and 5th Forum on New Materials Montecatini Terme, Italy, June 6-11, 2010 by Edited by Pietro VINCENZINI World Academy of Ceramics and National Research Council, Italy Co-edited by Michele DONDI CNR-ISTEC, Italy